Crystal Growth and Characterization of 1-(2,4- Dichlorophenyl-2yl)-3-(4-hydroxyphenyl)prop-2-en-1-one

Shubhalaxmi, . and Hahne, Stephanie and Jayarama, A and Bhat, Subrahmanya K (2013) Crystal Growth and Characterization of 1-(2,4- Dichlorophenyl-2yl)-3-(4-hydroxyphenyl)prop-2-en-1-one. Chemical Science Transactions, 2 (3). pp. 829-834. ISSN 2278-3318

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A potential crystal for nonlinear optical application and monomer namely 1-(2,4-dichlorophenyl-2yl)-3-(4-hydroxyphenyl)prop-2-en-1-one (DHPP) was synthesized and grown by slow evaporation technique. The functional groups present in the compound were identified by FTIR spectrum. The optical cut-off wavelength and structural characteristics were analyzed using UV-Vis-NIR spectra and single crystal x-ray diffractometer. The crystal belongs to non centrosymmetric orthorhombic system with space group Pna21 with cell parameters a= 18.015(3) Å, b= 18.218(3)Å,c= 4.1029(6) Å, Z=4 and V= 1346.56Å3. Thermal studies show that the crystal is stable up to 250 0C implying good processability

Item Type: Article
Uncontrolled Keywords: Hydroxychalcone, Crystal growth, Single crystal studies, X-ray diffraction
Subjects: Engineering > MIT Manipal > Chemistry
Depositing User: MIT Library
Date Deposited: 21 Sep 2013 06:04
Last Modified: 21 Sep 2013 06:12

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