Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2 hydroxy-4-methoxyphenyl)prop-2-en-1-one

Thippeswamy, GB and Vijaykumar, D and Mahadeva Prasad, TN and Jayashree, BS and Lakshminarayana, BN and Sridhar, MA and Shashidhara Prasad, J (2011) Synthesis and Crystal Structure of 3-(4-Ethylphenyl)-1-(2 hydroxy-4-methoxyphenyl)prop-2-en-1-one. X-ray Structure Analysis Online, 27. pp. 39-40.

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Abstract

The compound, 3-(4-ethylphenyl)-1-(2-hydroxy-4-methoxyphenyl)prop-2-en-1-one, was synthesized by using 4-methoxy-2-hydroxyacetophenone and 4-ethylbenzaldehyde solutions. The synthesized compound was characterized by spectroscopic techniques, and finally confirmed by X-ray diffraction studies. The compound is a dimer in nature, and crystallizes in the triclinic crystal class in the space group P1. The cell parameters are a = 9.6860(9)Å, b = 12.6650(17)Å,c = 13.4990(18)Å, a = 68.808(4)˚, b = 81.149(7)˚, g = 79.863(7)˚, V = 1511.5(3)˚ and Z = 4. In the crystal, O–H·O hydrogen bonds connect the hydroxy donor group and the C=O acceptor group. The R1[I > 2s(I)] and wR2 (all data) values are 0.0600 and 0.1984, respectively.

Item Type: Article
Subjects: Pharmacy > MCOPS Manipal > Pharmaceutical Chemistry
Depositing User: KMC Manipal
Date Deposited: 30 Jan 2012 10:31
Last Modified: 30 Jan 2012 10:31
URI: http://eprints.manipal.edu/id/eprint/2760

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